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5-Methoxyindole

CAS No.
1006-94-6
Chemical Name:
5-Methoxyindole
Synonyms
5-METHOXY-1H-INDOLE;Methoxyindole 99% indol-5-yl methyl ether;5-methoxy-indol;Femedol;NSC 521752;AKOS JY2082918;5-METHOXYINDOLE;methoxy-5indole;5-MethoxyindoleF;Methoxy-5 indole
CBNumber:
CB4223553
Molecular Formula:
C9H9NO
Molecular Weight:
147.17
MDL Number:
MFCD00005674
MOL File:
1006-94-6.mol
MSDS File:
SDS
Last updated:2024-11-16 17:07:08

5-Methoxyindole Properties

Melting point 52-55 °C (lit.)
Boiling point 176-178 °C/17 mmHg (lit.)
Density 1.1135 (rough estimate)
refractive index 1.5310 (estimate)
Flash point 176-178°C/17mm
storage temp. Keep in dark place,Sealed in dry,Room Temperature
solubility Chloroform, Methanol
form Crystalline Powder
pka 16.70±0.30(Predicted)
color White to light brownish
Water Solubility insoluble
Sensitive Light Sensitive
BRN 116722
InChIKey DWAQDRSOVMLGRQ-UHFFFAOYSA-N
CAS DataBase Reference 1006-94-6(CAS DataBase Reference)
EWG's Food Scores
FDA UNII
NIST Chemistry Reference

SAFETY

Risk and Safety Statements

Symbol(GHS)  trực tiếp đá gà hôm nayLiên kết đăng nhập
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P261-P264-P271-P280-P302+P352-P305+P351+P338
Hazard Codes  Xi
Risk Statements  36/37/38
Safety Statements  26-36-24/25-37/39
WGK Germany  3
RTECS  NL9500000
8
Hazard Note  Irritant
HazardClass  IRRITANT, KEEP COLD, LIGHT SENSITIVE
HS Code  29339900
NFPA 704
1
2 0

5-Methoxyindole price More Price(31)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich M14900 5-Methoxyindole 99% 1006-94-6 1g $25 2024-06-20 Buy
Sigma-Aldrich M14900 5-Methoxyindole 99% 1006-94-6 5g $34 2024-06-20 Buy
TCI Chemical M0731 5-Methoxyindole >99.0%(GC) 1006-94-6 1g $32 2024-06-20 Buy
TCI Chemical M0731 5-Methoxyindole >99.0%(GC) 1006-94-6 5g $55 2024-06-20 Buy
Alfa Aesar B25290 5-Methoxyindole, 99% 1006-94-6 1g $41 2024-06-20 Buy
Product number Packaging Price Buy
M14900 1g $25 Buy
M14900 5g $34 Buy
M0731 1g $32 Buy
M0731 5g $55 Buy
B25290 1g $41 Buy

5-Methoxyindole Chemical Properties,Uses,Production

Chemical Properties

white to light brownish crystalline powder

Uses

5-Methoxyindole (cas# 1006-94-6) is a compound useful in organic synthesis. It can be used to synthesis 1-(Phenylsulfonyl)-5-methoxy-1H-indole.

Definition

ChEBI: 5-methoxyindole is a member of indoles.

Preparation

The synthesis of 5-methoxyindole from 5-methoxy-2-oxindole: Conversion of 5-methoxy-2-oxindole to 5-methoxyindole was accomplishedby the chlorination of 5-methoxy-2-oxindole with triphenylphosphine-carbontetrachloride in acetonitrile followed by the catalytic reduction of a chlorine atom in 66% total yield.

Reactions

5-methoxyindole was treated with sodium hydroxide and phenylsulfonyl chloride in the presence of a catalytic amount of tetrabutylammonium bromide to afford 1-(phenylsulfonyl)indole and 5-methoxy-1-(phenylsufonyl)indole in excellent yields of 100%.

Synthesis Reference(s)

Journal of Heterocyclic Chemistry, 26, p. 1405, 1989 DOI:
The Journal of Organic Chemistry, 58, p. 5558, 1993 DOI:
Tetrahedron Letters, 27, p. 837, 1986 DOI:

Purification Methods

Crystallise 5-methoxyindole from cyclohexane pet ether or pet ether/Et2O. [Saito & Kikugawa J Heterocycl Chem 16 1325 1979, Beilstein 21 III/IV 765, 21/3 V 18.]
845619-77-4
1006-94-6
Synthesis of 5-Methoxyindole from 1-Propanone, 1-(5-methoxy-1H-indol-1-yl)-2,2-dimethyl-
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View Lastest Price from 5-Methoxyindole manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
trực tiếp đá gà hôm nayLiên kết đăng nhập 2024-12-19 5-Methoxyindole
1006-94-6
US $129.00-645.00 / g 1g 0.99 25kg Shanghai UCHEM Inc.
trực tiếp đá gà hôm nayLiên kết đăng nhập 2024-07-25 5-Methoxyindole
1006-94-6
US $20.00-10.00 / kg 1kg 99% 2T Hebei Yanxi Chemical Co., Ltd.
trực tiếp đá gà hôm nayLiên kết đăng nhập 2024-03-27 5-Methoxyindole
1006-94-6
US $25.00 / KG 1KG 0.99 5000KG/MONTH XINGTAI XINGJIU NEW MATERIAL TECHNOLOGY CO., LTD
  • trực tiếp đá gà hôm nayLiên kết đăng nhập
  • 5-Methoxyindole
    1006-94-6
  • US $20.00-10.00 / kg
  • 99%
  • Hebei Yanxi Chemical Co., Ltd.
  • trực tiếp đá gà hôm nayLiên kết đăng nhập
  • 5-Methoxyindole
    1006-94-6
  • US $25.00 / KG
  • 0.99
  • XINGTAI XINGJIU NEW MATERIAL TECHNOLOGY CO., LTD
5-Methoxyindole ,98% 5-METHOXYINDOLE (5MeOI) 5-methoxy-1H-indole(SALTDATA: FREE) 5-MethoxyindoleF 5-METHOXYINDOLE REPANIDAL NSC 521752 5-METHOXYINDOLE AKOS JY2082918 RARECHEM AH BS 0117 TIMTEC-BB SBB004094 1H-Indol-5-yl methyl ether Femedol Indole, 5-methoxy- Methoxy-5 indole methoxy-5indole 5-Methyoxy Indole 5-methyloxyl indole 5-Methoxylindole Methoxyindole,99% Indol-5-yl methyl ether 5-Methoxyindole in stock Factory 5-Methoxyindole> 5-Methoxyindole 1006-94-6 Methoxyindole 99% indol-5-yl methyl ether 5-METHOXY-1H-INDOLE 5-methoxy-indol 1006-94-6 Indoles Simple Indoles Building Blocks Heterocyclic Building Blocks blocks IndolesOxindoles Heterocycles Indoles and derivatives IndoleDerivative Pyrroles & Indoles Heterocyclic Compounds Indole Series Indoles Indoline & Oxindole Indole Building Blocks C7 to C9 Chemical Synthesis Heterocyclic Building Blocks Heterocycle-Indole series Indole Derivatives Simple Indoles Chiral Compound Pyrroles & Indoles Building Blocks Heterocyclic Building Blocks
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